以三氯氧磷和2,2,2-三氟乙醇为原料是工业化使用较多的方法,但原料2,2,2-三氟乙醇成本高,存在较大改进空间.

磷酸三(2,2,2三氟乙基)酯的合成方法,属于电池电解液添加剂的技术领域,于氮气保护下,以三氟乙醇为原料,与缚酸剂加入到溶剂中,然后加入三氯氧磷进行反应,所得反应液抽滤后,经洗涤,干燥,脱色,浓缩得到磷酸三(2,2,2三氟乙基)酯,

目前还没看到气相色谱法测定磷酸三(2,2,2三氟乙基)酯的报道，浩瀚色谱（山东）应用技术开发有限公司，研制《磷酸三(2,2,2-三氟乙基)酯测定气相色谱仪 》，，建立了磷酸三(2,2,2-三氟乙基)酯的分析方法，纯度及杂质得到有效分离，合成产物的收率高、纯度高达99.95%。
 

浩瀚色谱，变不可能为可能。根据用户的要求，建立分析方案

​

名称：毛细管柱

规格：30m*0.32mm*0.5um

型号：HH-TTFPa

应用：工业磷酸三(2,2,2-三氟乙基)酯纯度及杂质测定  气相色谱法

 

Using phosphorus oxychloride and 2,2,2-trifluoroethanol as raw materials is a commonly employed industrial method, but the high cost of 2,2,2-trifluoroethanol leaves significant room for improvement
A synthesis method of tris(2,2,2-trifluoroethyl) phosphate, belonging to the technical field of battery electrolyte additives, involves protecting with nitrogen, using trifluoroethanol as the raw material, adding it to a solvent along with a base, then reacting with phosphorus oxychloride. The resulting reaction mixture is filtered, washed, dried, decolorized, and concentrated to obtain tris(2,2,2-trifluoroethyl) phosphate,
There are currently no reports on the determination of tris(2,2,2-trifluoroethyl) phosphate by gas chromatography. Haohan Chromatography (Shandong) Application Technology Co., Ltd. has developed a "Gas Chromatograph for the Determination of Tris(2,2,2-trifluoroethyl) Phosphate," establishing an analytical method for tris(2,2,2-trifluoroethyl) phosphate. The purity and impurities are effectively separated, with the synthetic product exhibiting high yield and purity reaching 99.95%.
In the vast realm of chromatography, the impossible becomes possible. Based on the user's requirements, an analytical solution is established
​
Name: Capillary Column
Specifications: 30m * 0.32mm * 0.5um
Model: HH-TTFPa
Application: Determination of Purity and Impurities in Industrial Tri(2,2,2-Trifluoroethyl) Phosphate by Gas Chromatography